Equipe Microstructures de Croissance Auto-organisées
Self-organized Growth Microstructures Team

Adresse :
IM2NP
Faculté des Sciences et Techniques
Aile 1 - niveau 4, service 141
Avenue Escadrille Normandie Niemen
13397 Marseille Cedex 20
France
Radiographie enregistrée lors de la croissance de dendrites colonnaires.(alliage : Al – 3,5 % pds Ni ; G = 7 K/cm ; V = 40 µm/s)
Expérience réalisée à l’ESRF (European Synchrotron Radiation Facility) Grenoble.
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Films : microstructures de solidification

Columnar_AlNi.avi

In situ and real-time observation by X-ray radiography of the initial transient during non refined Al-3.5wt% Ni solidification, G = 20 K/cm. Solidification was induced by pulling the sample toward the cold zone of the furnace at V = 1 mm/s. The aluminium rich solidified part appears in grey while the Ni enriched liquid is dark.
Expérience réalisée à l’ESRF, Grenoble

Columnar_SCN-Camphre.avi

In situ and real-time observation of columnar dendritic solidification in a SCN-0.1wt%Camphor alloy (G = 17 K/cm ; V = 20 µm/s).  Multiple and continuous tip-splittings of dendrites


CET AlNi

CET_AlNi.avi

In situ and real-time observation by X-ray radiography of the columnar to Equiaxed Transition (CET) during refined Al-3.5wt% Ni solidification, G = 30 K/cm. CET was induced by increasing the pulling rate from V = 2 to 15 mm/s. The aluminium rich solidified parts appear in grey while the Ni enriched liquid is dark.
Expérience réalisée à l’ESRF, Grenoble


CET_SCN-H2O_1
CET_SCN-H2O_1

In situ and real-time observation by the Columnar to Equiaxed Transition (CET) during downward solidification of a Succinonitrile-29wt%H2O alloy. CET was induced by the gradual increase of the pulling rate, due to the imposed decrease of the temperature of furnace hot zone. In "CET_SCN-H2O_1", fragmentations of the dendritic branches occur in the columnar area (top zone) and the fragments are driven away by convection and are used to nucleate the equiaxed grains.


Equiaxed_AlCu10_iso1

Equiaxed_AlCu10_iso1.avi

In situ and real-time observation by X-ray radiography of the equiaxed growth in nearly isothermal conditions of non-refined Al-10wt% Cu alloy. Solidification was induced by decreasing the temperatures of hot and cold zones of the furnace at R =  0.5 K/min. The solid parts mainly constituted of aluminium appear in white while the Cu enriched liquid is dark.
Expérience réalisée à l’ESRF, Grenoble

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